N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

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Chemical Name:N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine
CAS No.:1329602-88-1
Molecular Formula:C₂₂H₃₂N₂O₈S
Molecular Weight:484.571
Hs Code.:

Synonyms:N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

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Chemical Property of N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

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Technology Process of N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

There total 3 articles about N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1329602-89-2
C₂₈H₃₈N₂O₁₁S

: 1329602-88-1
N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Guidance literature:: With methanol; sodium methylate; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1ob05573a

Reference yield:

: 10154-71-9
3-(phenylsulfonyl)propionic acid

: 1329602-88-1
N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / toluene / 3 h / Reflux; Inert atmosphere

2: triethylamine / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

3: methanol; sodium methylate / 20 °C / Inert atmosphere

With methanol; oxalyl dichloride; sodium methylate; triethylamine; In tetrahydrofuran; toluene; 3: Zemplen deprotection;
DOI:10.1039/c1ob05573a

Reference yield:

: 3445-53-2
3-(benzenesulphonyl)propionyl chloride

: 1329602-88-1
N-[(1S,2R)-2-(3-(phenylsulfonyl)propanamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

2: methanol; sodium methylate / 20 °C / Inert atmosphere

With methanol; sodium methylate; triethylamine; In tetrahydrofuran; 2: Zemplen deprotection;
DOI:10.1039/c1ob05573a