3-(PHENYLSULFONYL)PROPIONIC ACID

Base Information

• Chemical Name: 3-(PHENYLSULFONYL)PROPIONIC ACID
• CAS No.: 10154-71-9
• Molecular Formula: C9H10O4S
• Molecular Weight: 214.242
• Hs Code.: 2916399090
• Mol file: 10154-71-9.mol

Synonyms:ART-CHEM-BB B022233;IFLAB-BB F0266-3532;AKOS B022233;3-BENZENESULFONYL-PROPIONIC ACID;3-(PHENYLSULFONYL)PROPIONIC ACID;OTAVA-BB BB0112820087;3-(phenylsulphonyl)propionic acid;3-(PHENYLSULFONYL)PROPIONIC ACID 99%

Chemical Property of 3-(PHENYLSULFONYL)PROPIONIC ACID

Chemical Property:

• Vapor Pressure: 3.23E-09mmHg at 25°C
• Melting Point: 128-130°C
• Refractive Index: 1.556
• Boiling Point: 458.9°Cat760mmHg
• PKA: 3.85±0.10(Predicted)
• Flash Point: 231.4°C
• PSA: 79.82000
• Density: 1.348g/cm³
• LogP: 2.01580
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: methanol: soluble25mg/mL, clear, colorless

Purity/Quality:

97% ^*data from raw suppliers

3-(Phenylsulfonyl)propanoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-(Phenylsulfonyl)propionic acid may be used in chemical synthesis.

Technology Process of 3-(PHENYLSULFONYL)PROPIONIC ACID

There total 27 articles about 3-(PHENYLSULFONYL)PROPIONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

acrylic acid (79-10-7) + phenylboronic acid (98-80-6) → 3-(phenylsulfonyl)propionic acid (10154-71-9)

Guidance literature:

With acetamide; sodium metabisulfite; C₂₃H₃₁NP⁽¹⁺⁾*Cl^(1-); choline chloride; palladium dichloride; at 80 ℃; for 24h; Green chemistry;

DOI:10.1002/chem.201702892

Reference yield: 83.0%

acrylic acid (79-10-7) + benzenesufonyl hydrazide (80-17-1) → 3-(phenylsulfonyl)propionic acid (10154-71-9)

Guidance literature:

In water; at 120 ℃; for 24h; Sealed tube;

Reference yield: 80.0%

triphenylbismuthane (603-33-8) + acrylic acid (79-10-7) → 3-(phenylsulfonyl)propionic acid (10154-71-9)

Guidance literature:

With acetamide; sodium metabisulfite; acetylcholine chloride; at 80 ℃; for 5h;

DOI:10.1002/ejoc.202000425

upstream raw materials:

β-Propiolactone

acide phenylthio-3 propanoique

3-benzenesulfonyl-propionitrile

sodium 3-chloroproanoate

Downstream raw materials:

3-(phenylsulfonyl)propanamide

1-Brom-4-benzolsulfonyl-butanon-⁽²⁾

acrylic acid

Benzenesulfinic acid