3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

Base Information

Chemical Name:3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal
CAS No.:862378-18-5
Molecular Formula:C₂₂H₂₂O₅S₄
Molecular Weight:494.678
Hs Code.:

Synonyms:3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

Suppliers and Price of 3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

There total 2 articles about 3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 7404-42-4
D-Mannose-dibenzyldithioacetal

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 2-O-imidazolylthiocarbonyl-3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

: 862378-18-5
3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

Guidance literature:: In 1,4-dioxane; at 20 ℃;
DOI:10.1016/j.tet.2005.05.008

Reference yield: 23.0%

: 7404-42-4
D-Mannose-dibenzyldithioacetal

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 862378-18-5
3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

: Imidazole-1-carbothioic acid O-[(S)-2,2-bis-benzylsulfanyl-1-((4R,5S,4'R)-2,2'-dithioxo-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl] ester

Guidance literature:: In 1,4-dioxane; at 20 ℃;
DOI:10.1016/j.tetlet.2004.03.197

Reference yield: 36.0%

: 108-24-7
acetic anhydride

: 862378-18-5
3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal

: 2,4,5,-tri-O-acetyl-3,6-thioanhydro-D-allose dibenzyl dithioacetal

Guidance literature:: 3,4:5,6-di-O-thiocarbonyl-D-mannose dibenzyl dithioacetal; With sodium sulfide; In dimethyl sulfoxide; at 80 ℃; for 1h;

acetic anhydride; In pyridine; Further stages.;
DOI:10.1016/j.tetlet.2004.03.197