benzhydryl 1-propynyl sulfone

Base Information

Chemical Name:benzhydryl 1-propynyl sulfone
CAS No.:1334033-13-4
Molecular Formula:C₁₆H₁₄O₂S
Molecular Weight:270.352
Hs Code.:

Synonyms:benzhydryl 1-propynyl sulfone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzhydryl 1-propynyl sulfone

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Technology Process of benzhydryl 1-propynyl sulfone

There total 2 articles about benzhydryl 1-propynyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1334032-63-1
benzhydryl 1-propynyl sulfide

: 1334033-13-4
benzhydryl 1-propynyl sulfone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 6 ℃; Inert atmosphere;
DOI:10.1021/ol202196y

Reference yield:

: 776-74-9
Bromodiphenylmethane

: 1334033-13-4
benzhydryl 1-propynyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 6 °C / Inert atmosphere

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol202196y