4-formylantipyrine thiosemicarbazone

Base Information

• Chemical Name: 4-formylantipyrine thiosemicarbazone
• CAS No.: 96715-43-4
• Molecular Formula: C₁₃H₁₅N₅OS
• Molecular Weight: 289.361
• Mol file: 96715-43-4.mol

Synonyms:4-formylantipyrine thiosemicarbazone

Chemical Property of 4-formylantipyrine thiosemicarbazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 4-formylantipyrine thiosemicarbazone

There total 1 articles about 4-formylantipyrine thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-formyl-2,3-dimethyl-1-phenyl-3-pyrazolin-5-one (950-81-2) + thiosemicarbazide (79-19-6) → 4-formylantipyrine thiosemicarbazone (96715-43-4)

Guidance literature:

In neat (no solvent); at 20 ℃; for 1h; Milling; Green chemistry;

DOI:10.3390/molecules201219820

Reference yield: 100.0%

4-formylantipyrine thiosemicarbazone (96715-43-4) + α-bromoacetophenone (70-11-1) → 2-(antipyrin-4-ylmethylidenehydrazinyl)-4-phenylthiazole hydrobromide

Guidance literature:

In neat (no solvent); at 20 ℃; for 1h; Milling; Green chemistry;

DOI:10.3390/molecules201219820

Reference yield: 98.0%

4-formylantipyrine thiosemicarbazone (96715-43-4) + α-bromoacetophenone (70-11-1) → 2-(antipyrin-4-ylmethylidenehydrazinyl)-4-phenylthiazole (100259-94-7)

Guidance literature:

4-formylantipyrine thiosemicarbazone; α-bromoacetophenone; In neat (no solvent); at 20 ℃; for 1h; Milling; Green chemistry;

With sodium carbonate; Green chemistry;

DOI:10.3390/molecules201219820

upstream raw materials:

4-formyl-2,3-dimethyl-1-phenyl-3-pyrazolin-5-one

thiosemicarbazide

Downstream raw materials:

[copper(II)(4-formylantipyrine thiosemicarbazone)(C₁₃H₁₄N₅OS)]BF₄

Fe(C₁₃H₁₄N₅OS)2⁽¹⁺⁾*ClO₄^(1-)=[Fe(C₁₃H₁₄N₅OS)2]ClO₄

[nickel(II)(4-formylantipyrine thiosemicarbazone)(C₁₃H₁₄N₅OS)(CH₃COO)] monohydrate

[Co(C₁₃H₁₄N₅OS)(CH₃COO)]2