methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside

Base Information

Chemical Name:methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside
CAS No.:182804-38-2
Molecular Formula:C₄₁H₄₀O₁₃
Molecular Weight:740.761
Hs Code.:

Synonyms:methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside

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Technology Process of methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside

There total 6 articles about methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₃H₄₄O₁₃

: 182804-38-2
methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: With acetic acid; In N,N-dimethyl-formamide; for 1h; Yield given;

Reference yield:

: 131897-73-9
2,3,4-tri-O-benzoyl-α-L-fucopyranosyl bromide

: 182804-38-2
methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: Hg(CN)2, HgBr₂, molecular sieves 4 Angstroem / acetonitrile / 1 h

2: 90percent aq. CF₃COOH / 1 h

3: TsOH / H₂O; dimethylformamide / 3 h / Ambient temperature

4: 90percent aq. acetic acid / dimethylformamide / 1 h

With 4 A molecular sieve; mercury(II) cyanide; toluene-4-sulfonic acid; acetic acid; trifluoroacetic acid; mercury dibromide; In water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1663-61-2
triethoxymethylbenzene

: 182804-38-2
methyl 2-O-benzoyl-4-O-(2,3,4-tri-O-benzoyl-β-L-fucopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: TsOH / H₂O; dimethylformamide / 3 h / Ambient temperature

2: 90percent aq. acetic acid / dimethylformamide / 1 h

With toluene-4-sulfonic acid; acetic acid; In water; N,N-dimethyl-formamide;