methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride

Base Information

Chemical Name:methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride
CAS No.:1613396-72-7
Molecular Formula:C₁₄H₁₄Cl₂N₂O₂
Molecular Weight:313.183
Hs Code.:

Synonyms:methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride

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Chemical Property of methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride

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Technology Process of methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride

There total 4 articles about methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613396-71-6
methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carboxylic acid

: 1613396-72-7
methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; for 3h;

Reference yield:

: 42558-54-3
Methyl 4-methyl-3-oxopentanoate

: 1613396-72-7
methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 24 h / 100 °C

2: N,N-dimethyl-formamide / 8 h / 100 °C

3: lithium hydroxide monohydrate; water / tetrahydrofuran / 1.5 h / 60 °C

4: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h

With oxalyl dichloride; lithium hydroxide monohydrate; water; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1613396-67-0
methyl (2Z)-2-(dimethylaminomethylene)-4-methyl-3-oxo-pentanoate

: 1613396-72-7
methyl 1-(4-chloro-3-methoxyphenyl)-5-isopropylpyrazole-4-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 8 h / 100 °C

2: lithium hydroxide monohydrate; water / tetrahydrofuran / 1.5 h / 60 °C

3: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h

With oxalyl dichloride; lithium hydroxide monohydrate; water; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;