N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide
CAS No.:1579268-82-8
Molecular Formula:C₃₄H₃₆N₂O₇S₂
Molecular Weight:648.801
Hs Code.:

Synonyms:N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

Suppliers and Price of N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1378478-43-3
C₁₈H₂₁NO₄S

: 139717-71-8
5-methoxy-N-(4-toluenesulfonyl)-1H-indole

: 1579268-82-8
N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

Guidance literature:: 5-methoxy-N-(4-toluenesulfonyl)-1H-indole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

C₁₈H₂₁NO₄S; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;
DOI:10.1016/j.tet.2014.01.074

Reference yield: 89.0%

: 1579268-82-8
N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

: 1579269-06-9
9-methoxy-5-(4-methoxyphenyl)-2,6-ditosyl-1,2,3,4,5,6-hexahydroazepino[4,3-b]indole

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/j.tet.2014.01.074

Reference yield:

: 1579268-82-8
N-(3-hydroxy-3-(5-methoxy-1-tosyl-1H-indol-2-yl)propyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

: 1579269-23-0
5-(4-methoxyphenyl)-6-tosyl-1,2,3,4,5,6-hexahydroazepino[4,3-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 0 °C

2: potassium carbonate; thiophenol / N,N-dimethyl-formamide / 1.5 h / 20 °C

With potassium carbonate; thiophenol; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2014.01.074