methyl 1-deuteriocyclohexanecarboxylate

Base Information

Chemical Name:methyl 1-deuteriocyclohexanecarboxylate
CAS No.:1206201-75-3
Molecular Formula:C₈H₁₄O₂
Molecular Weight:143.19
Hs Code.:

Synonyms:methyl 1-deuteriocyclohexanecarboxylate

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Chemical Property of methyl 1-deuteriocyclohexanecarboxylate

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Technology Process of methyl 1-deuteriocyclohexanecarboxylate

There total 2 articles about methyl 1-deuteriocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 933-37-9
1-deuterio-cyclohexanecarboxylic acid

: 74-88-4
methyl iodide

: 1206201-75-3
methyl 1-deuteriocyclohexanecarboxylate

Guidance literature:: 1-deuterio-cyclohexanecarboxylic acid; With potassium hydroxide; In dimethyl sulfoxide; for 0.0833333h;

methyl iodide; In dimethyl sulfoxide; at 20 ℃;

Reference yield:

: 4630-82-4
methyl cyclohexylcarboxylate

: 1206201-75-3
methyl 1-deuteriocyclohexanecarboxylate

Guidance literature:: methyl cyclohexylcarboxylate; With lithium diisopropyl amide; In tetrahydrofuran; at -70 - 20 ℃; Inert atmosphere;

With water-d2; In tetrahydrofuran; at -70 - 20 ℃; Inert atmosphere;
DOI:10.1021/jp9073398

Reference yield: 97.0%

: 1206201-75-3
methyl 1-deuteriocyclohexanecarboxylate

: 1222168-12-8
[1-⁽²⁾H₁]-cyclohexylmethanol

Guidance literature:: methyl 1-deuteriocyclohexanecarboxylate; With diisobutylaluminium hydride; In dichloromethane; at 20 ℃; for 2h; Ice bath;

With water; rochelle salt; In dichloromethane;