Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

Base Information

• Chemical Name: Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane
• CAS No.: 161584-85-6
• Molecular Formula: C₃₀H₃₈N₂O₄Si
• Molecular Weight: 518.728

Synonyms:Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

Chemical Property of Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane

There total 1 articles about Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl bromide (74-96-4) + Bis(6-cyano-2-pyridyl)methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane → Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane (161584-85-6)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) benzene, Et₂O, r.t., 2.) benzene, r.t., 1.5 h;

DOI:10.1021/jo00111a038

Reference yield:

Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane (161584-85-6) → 1-(6-{[4-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-[6-(1-hydroxy-propyl)-pyridin-2-yl]-methoxy-methyl}-pyridin-2-yl)-propan-1-ol

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 40 ℃; for 5h;

DOI:10.1021/jo00111a038

Reference yield:

Bis<6-(1-oxopropyl)-2-pyridyl>methoxy<4-((tert-butyldimethylsilyl)oxy)phenyl>methane (161584-85-6) → (R)-1-(6-{[4-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-[6-((R)-1-hydroxy-propyl)-pyridin-2-yl]-methoxy-methyl}-pyridin-2-yl)-propan-1-ol

Guidance literature:

With (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; for 48h; Ambient temperature;

DOI:10.1021/jo00111a038

upstream raw materials:

ethyl bromide

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