1D-(1,2,4,5S/3,5C)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol

Base Information

Chemical Name:1D-(1,2,4,5S/3,5C)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol
CAS No.:108032-89-9
Molecular Formula:C₃₇H₄₀O₆S
Molecular Weight:612.787
Hs Code.:

Synonyms:1D-(1,2,4,5S/3,5C)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol

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Chemical Property of 1D-(1,2,4,5S/3,5C)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol

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Technology Process of 1D-(1,2,4,5S/3,5C)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol

There total 6 articles about 1D-(1,2,4,5S/3,5C)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 613-90-1
benzoyl cyanide

: 107960-18-9,110453-99-1
(2S,3R,4S,5S)-2,3,4-Tris-benzyloxy-5-ethylsulfanyl-5-hydroxymethyl-cyclohexanol

: C₄₂H₃₄O₁₀

: 108032-89-9
1D-(1,2,4,5S/3,5C)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol

: 107960-19-0,108032-89-9
Benzoic acid (1S,2S,3R,4S,5R)-2,3,4-tris-benzyloxy-1-ethylsulfanyl-5-hydroxy-cyclohexylmethyl ester

Guidance literature:: With triethylamine; In acetonitrile; at -15 ℃;

Reference yield: 73.0%

: 613-90-1
benzoyl cyanide

: 107960-18-9,110453-99-1
(2S,3R,4S,5S)-2,3,4-Tris-benzyloxy-5-ethylsulfanyl-5-hydroxymethyl-cyclohexanol

: C₄₂H₃₄O₁₀

: 108032-89-9
1D-(1,2,4,5S/3,5C)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol

: 107960-19-0,108032-89-9
Benzoic acid (1S,2S,3R,4S,5R)-2,3,4-tris-benzyloxy-1-ethylsulfanyl-5-hydroxy-cyclohexylmethyl ester

Guidance literature:: With triethylamine; In acetonitrile; at -15 ℃;

Reference yield:

: 107960-16-7,108032-87-7
1L-(1S,2,4/1C,3)-5-O-Acetyl-2,3,4-tri-O-benzyl-1-C-(ethylthio)-2,3,4,5-tetrahydroxy-1-cyclohexancarbonitril

: 107960-19-0,108032-89-9
Benzoic acid (1S,2S,3R,4S)-2,3,4-tris-benzyloxy-1-ethylsulfanyl-5-hydroxy-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / DIBAH / CH₂Cl₂; petroleum ether / -70 - 25 °C

2: 1) LiAlH₄, 2) NEt₃ / 1) THF, 0 deg C to r.t., 2) CH₃CN, -15 deg C

With lithium aluminium tetrahydride; diisobutylaluminium hydride; triethylamine; In dichloromethane; Petroleum ether;