1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

Base Information

Chemical Name:1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen
CAS No.:75348-20-8
Molecular Formula:C₃₅H₃₄O₆
Molecular Weight:550.651
Hs Code.:

Synonyms:1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

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Chemical Property of 1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

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Technology Process of 1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

There total 19 articles about 1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 613-90-1
benzoyl cyanide

: 75348-19-5
1L-(1,2/2,4)-2,3,4-Tri-O-benzyl-5-C-(hydroxymethyl)-5-cyclohexen-1,2,3,4-tetrol

: 75348-20-8
1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

Guidance literature:: With triethylamine; In acetonitrile; at -15 ℃;

Reference yield: 53.0%

: 110372-71-9
2D-(2,4/3)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-2,3,4-trihydroxy-5-cyclohexen-1-on

: 75348-20-8
1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

: 110454-00-7
1D-(1,2,4/3)-5-C-(Benzoyloxy)methyl-2,3,4-tri-O-benzyl-5-cyclohexen-1,2,3,4-tetrol

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In methanol; Ambient temperature;

Reference yield:

: 75251-60-4,75419-03-3
1L-1,7-Anhydro-1-C-hydroxymethyl-3,4:5,6-di-O-isopropyliden-2-O-methyl-chiro-inosit

: 75348-20-8
1L-(1,3/2,4)-7-O-Benzoyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

Guidance literature:: Multi-step reaction with 11 steps

1: 89 percent / H₂O, alkaline

2: BBr₃

4: H₂O

5: 75 percent

6: H₂O, acid

7: 82 percent

9: 1) NaI, 2) POCl₃

10: H₂O

With Alkaline; water; boron tribromide; sodium iodide; trichlorophosphate;