((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(C₆H₅CCH)(⁽¹³⁾CO)3

Base Information

Chemical Name:((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(C₆H₅CCH)(⁽¹³⁾CO)3
CAS No.:96481-29-7
Molecular Formula:C₃₇H₃₀O₃P₂W
Molecular Weight:771.408
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)W(C<sub>6</sub>H<sub>5</sub>CCH)(<sup>(13)</sup>CO)3

Synonyms:((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(C₆H₅CCH)(⁽¹³⁾CO)3

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Chemical Property of ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(C₆H₅CCH)(⁽¹³⁾CO)3

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Technology Process of ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(C₆H₅CCH)(⁽¹³⁾CO)3

There total 2 articles about ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(C₆H₅CCH)(⁽¹³⁾CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96454-53-4
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(⁽¹³⁾CO)3⁽¹⁺⁾*BF₄^(1-)=((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(⁽¹³⁾CO)3BF₄

: 96481-29-7
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(C₆H₅CCH)(⁽¹³⁾CO)3

Guidance literature:: With Al₂O₃; In dichloromethane; a soln. of the complex was cooled to 0°C, Al2O3 was added, the mixt. was stirred under N2 (IR monitoring), the soln. was sepd. from Al2O3 by extg., solvent was removed in vacuo, the green solid was extd. withtoluene and triturated with pentane; identified by IR and NMR spectra;
DOI:10.1021/ja00301a017

Reference yield:

: 98586-68-6
Li⁽¹⁺⁾*(OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCC₆H₅)^(1-)=Li((OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCC₆H₅))

: 1641-69-6
[13C]Carbon monoxide

: 88035-90-9
mer-bis(diphenylphosphino)ethane(carbonyl)3tungsten(CC(H)Ph)

: 96481-29-7
((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(C₆H₅CCH)(⁽¹³⁾CO)3

Guidance literature:: With HBF₄; In tetrahydrofuran; a soln. of W-complex was protonated under 1 atm (13)CO; no (13)CO was found in the vinylidene product;