benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester

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Chemical Name:benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester
CAS No.:180423-10-3
Molecular Formula:C₂₉H₃₁N₅O₅
Molecular Weight:529.596
Hs Code.:

Synonyms:benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester

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Chemical Property of benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester

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Technology Process of benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester

There total 5 articles about benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.7%

: 180423-10-3
benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester

Guidance literature:

Reference yield:

: 41406-00-2
3-isopropoxyaniline

: 180423-10-3
benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / 2 h / Ambient temperature

2: 72.1 percent / AcOH / 16 h / Heating

3: 88.4 percent / NH₂NH₂ / ethanol / 18 h / Heating

4: acetonitrile / 16 h / Ambient temperature

With acetic acid; triethylamine; hydrazine; In ethanol; acetonitrile;
DOI:10.1021/jm970373j

Reference yield:

: 3528-90-3
3-isopropoxy-phenyl isothiocyanate

: 180423-10-3
benzoic acid, 3-[[[2-[3,4-dihydro-3-[3-(1-methylethoxy)phenyl]-4-oxo-2-quinazolinyl]-hydrazino]carbonyl]amino]-, 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72.1 percent / AcOH / 16 h / Heating

2: 88.4 percent / NH₂NH₂ / ethanol / 18 h / Heating

3: acetonitrile / 16 h / Ambient temperature

With acetic acid; hydrazine; In ethanol; acetonitrile;
DOI:10.1021/jm970373j