Technology Process of C14H20O4
There total 6 articles about C14H20O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
at 0 - 20 ℃;
for 3h;
DOI:10.1055/s-0029-1217556
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium iodide; zinc / methanol / 3 h / Reflux
2: sodium hydride / tetrahydrofuran / 4 h / 0 - 20 °C
3: toluene-4-sulfonic acid / methanol / 3 h / 0 - 20 °C
With
sodium hydride; toluene-4-sulfonic acid; sodium iodide; zinc;
In
tetrahydrofuran; methanol;
DOI:10.1055/s-0029-1217556
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.17 h / 0 °C
2: sodium iodide; zinc / methanol / 3 h / Reflux
3: sodium hydride / tetrahydrofuran / 4 h / 0 - 20 °C
4: toluene-4-sulfonic acid / methanol / 3 h / 0 - 20 °C
With
1H-imidazole; iodine; sodium hydride; toluene-4-sulfonic acid; triphenylphosphine; sodium iodide; zinc;
In
tetrahydrofuran; methanol;
DOI:10.1055/s-0029-1217556