(S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester

Base Information

Chemical Name:(S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester
CAS No.:1189520-70-4
Molecular Formula:C₂₈H₃₆O₆
Molecular Weight:468.59
Hs Code.:

Synonyms:(S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester

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Chemical Property of (S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester

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Technology Process of (S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester

There total 17 articles about (S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1189520-71-5
(2R,4S)-4-(4-methoxy-benzyloxy)-hex-5-en-2-ol

: 1189520-72-6
(S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid

: 1189520-70-4
(S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester

Guidance literature:: (S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid; With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; at 20 ℃; for 0.5h;

(2R,4S)-4-(4-methoxy-benzyloxy)-hex-5-en-2-ol; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1016/j.tetasy.2009.10.007

Reference yield: 85.0%

: 1189520-71-5
(2R,4S)-4-(4-methoxy-benzyloxy)-hex-5-en-2-ol

: 1207564-27-9
(4R)-4-(4-methoxybenzyloxy)hex-5-enoic acid

: 1189520-70-4
(S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 14h;
DOI:10.1055/s-0029-1217556

Reference yield:

: (4R)-4-O-(4-methoxybenzyl)-hex-5-ene-1,4-diol

: 1189520-70-4
(S)-4-(4-methoxy-benzyloxy)-hex-5-enoic acid (1R,3S)-3-(4-methoxy-benzyloxy)-1-methyl-pent-4-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran; dimethyl sulfoxide / 3 h / 20 °C

2: sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; sodium perchlorate / water; tert-butyl alcohol / 2 h / 0 - 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 14 h / 0 °C

With dmap; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; sodium perchlorate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1055/s-0029-1217556