[Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine)(N,N'-di(p-tolyl)formamidine(-1H))]

Base Information

Chemical Name:[Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine)(N,N'-di(p-tolyl)formamidine(-1H))]
CAS No.:680224-06-0
Molecular Formula:C₃₅H₃₆MoN₄O₂
Molecular Weight:640.636
Hs Code.:

Synonyms:[Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine)(N,N'-di(p-tolyl)formamidine(-1H))]

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Chemical Property of [Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine)(N,N'-di(p-tolyl)formamidine(-1H))]

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Technology Process of [Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine)(N,N'-di(p-tolyl)formamidine(-1H))]

There total 1 articles about [Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine)(N,N'-di(p-tolyl)formamidine(-1H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 680224-01-5
[Mo(η(3)-allyl)Cl(CO)2(N,N'-di(p-tolyl)formamidine)2]

: 680224-06-0
[Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine)(N,N'-di(p-tolyl)formamidine(-1H))]

Guidance literature:: With CH₃CH₂CH₂CH₂Li; In tetrahydrofuran; hexane; under dry Ar or N2 atm. using Schlenk techniques; soln. of Mo complex inTHF cooled to -78°C; soln. of n-BuLi in hexane added; mixt. stir red at -78°C for 2 h; warmed to room temp.; after several hs volatiles removed (vac.); solid extd. (toluene); filtrate evapd. off (high vac.); residue washed (hexane); dried (vac.); elem. anal.;
DOI:10.1246/bcsj.77.303

Reference yield: 61.0%

: 680224-06-0
[Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine)(N,N'-di(p-tolyl)formamidine(-1H))]

: 554-70-1
triethylphosphine

: 680224-08-2
[Mo(η(3)-allyl)(CO)2(N,N'-di(p-tolyl)formamidine(-1H))(triethylphosphine)]

Guidance literature:: In dichloromethane; under dry Ar or N2 atm. using Schlenk techniques; to soln. of Mo complexin CH2Cl2 added PEt3 at room temp.; stirred for 1.5 h; volatiles removed (vac.); residue loaded on Al column and eluted with CH2Cl2/hexane (1/1 v/v %); the eluted red band collected; solvent removed (vac.); elem. anal.;
DOI:10.1246/bcsj.77.303