C₂₉H₂₄O₈

Base Information

Chemical Name:C₂₉H₂₄O₈
CAS No.:1229578-70-4
Molecular Formula:C₂₉H₂₄O₈
Molecular Weight:500.505
Hs Code.:

C<sub>29</sub>H<sub>24</sub>O<sub>8</sub>

Synonyms:C₂₉H₂₄O₈

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₄O₈

Chemical Property:

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Technology Process of C₂₉H₂₄O₈

There total 14 articles about C₂₉H₂₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1229578-69-1
C₄₅H₄₂O₁₀

: 1229578-70-4
C₂₉H₂₄O₈

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 0 - 20 ℃; for 2.5h; Cooling with ice;
DOI:10.1002/ejoc.201201339

Reference yield:

: 31721-94-5
5,7-dihydroxy-chromen-4-one

: 1229578-70-4
C₂₉H₂₄O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: calcium hydroxide / methanol / 72 h / 20 °C

2.1: potassium carbonate / acetone / 0.17 h / Cooling with ice

2.2: 3 h / Inert atmosphere; Reflux

3.1: methanol / 2 h / Reflux

4.1: pyridine; iodine / dichloromethane / 20 °C

5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water / 20 °C / Inert atmosphere

6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 2.5 h / 0 - 20 °C / Cooling with ice

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; iodine; sodium carbonate; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; calcium hydroxide; In methanol; dichloromethane; water; acetone; 5.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/ejoc.201201339

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 1229578-70-4
C₂₉H₂₄O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: boron trifluoride diethyl etherate; methanesulfonyl chloride / 3.83 h / 20 - 90 °C

2.1: calcium hydroxide / methanol / 72 h / 20 °C

3.1: potassium carbonate / acetone / 0.17 h / Cooling with ice

3.2: 3 h / Inert atmosphere; Reflux

4.1: methanol / 2 h / Reflux

5.1: pyridine; iodine / dichloromethane / 20 °C

6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water / 20 °C / Inert atmosphere

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 2.5 h / 0 - 20 °C / Cooling with ice

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; boron trifluoride diethyl etherate; iodine; sodium carbonate; potassium carbonate; methanesulfonyl chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; calcium hydroxide; In methanol; dichloromethane; water; acetone; 1.1: |Vilsmeier-Haack Formylation / 6.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/ejoc.201201339