(3R)-2-(tert-butoxycarbonyl)-7-hydroxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

Base Information

Chemical Name:(3R)-2-(tert-butoxycarbonyl)-7-hydroxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid
CAS No.:1187832-20-7
Molecular Formula:C₁₆H₂₁NO₅
Molecular Weight:307.346
Hs Code.:

Synonyms:(3R)-2-(tert-butoxycarbonyl)-7-hydroxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

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Chemical Property of (3R)-2-(tert-butoxycarbonyl)-7-hydroxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

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Technology Process of (3R)-2-(tert-butoxycarbonyl)-7-hydroxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

There total 6 articles about (3R)-2-(tert-butoxycarbonyl)-7-hydroxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1187832-18-3
(3R)-6,8-dibromo-7-methoxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

: 1187832-20-7
(3R)-2-(tert-butoxycarbonyl)-7-hydroxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

Guidance literature:: (3R)-6,8-dibromo-7-methoxy-3-methyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid; With hydrogen bromide; In water; for 5h; Reflux;

With hydrogen; triethylamine; palladium 10% on activated carbon; In methanol; for 12h; under 3863.02 Torr;

di-tert-butyl dicarbonate; With triethylamine; In water; N,N-dimethyl-formamide; for 10h;