10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane

Base Information

Chemical Name:10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane
CAS No.:143065-61-6
Molecular Formula:C₃₆H₅₈N₄O₁₀S₂
Molecular Weight:771.009
Hs Code.:

Synonyms:10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane

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Chemical Property of 10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane

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Technology Process of 10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane

There total 4 articles about 10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 143065-57-0
4-tosyl-10,13-bis(2-hydroxyethyl)-1,7-dioxa-4,10,13-triazacyclopentadecane

: 143065-61-6
10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 3h; Heating;
DOI:10.1021/jo00044a040

Reference yield:

: 4439-20-7
N,N'-bis(2-hydroxyethyl)ethylene diamine

: 143065-61-6
10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / Na₂CO₃ / acetonitrile / Heating

2: 80 percent / KOtBu / tetrahydrofuran / 3 h / Heating

With potassium tert-butylate; sodium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00044a040

Reference yield:

: 118187-55-6
N,N-bis<2-<2-<(p-tolylsulfonyl)oxy>ethoxy>ethyl>-p-toluenesulfonamide

: 143065-61-6
10,25-ditosyl-4,7,13,16,22,28-hexaoxa-1,10,19,25-tetraazabicyclo<17.11.2>dotriacontane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / Na₂CO₃ / acetonitrile / Heating

2: 80 percent / KOtBu / tetrahydrofuran / 3 h / Heating

With potassium tert-butylate; sodium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00044a040