ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate

Base Information

Chemical Name:ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate
CAS No.:1621392-92-4
Molecular Formula:C₂₀H₂₃NO₅
Molecular Weight:357.406
Hs Code.:

Synonyms:ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate

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Chemical Property of ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate

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Technology Process of ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate

There total 4 articles about ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1621392-99-1
ethyl 2-(benzamidomethyl)-3-(4-methoxyphenyl)-3-oxopropanoate

: 1621392-92-4
ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₉H₄₅FeN₂O₂PS; hydrogen; sodium acetate; In isopropyl alcohol; toluene; at 60 ℃; for 24h; under 26601.8 Torr; stereoselective reaction; Autoclave;
DOI:10.1002/adsc.202100929

Reference yield:

: 1621392-99-1
ethyl 2-(benzamidomethyl)-3-(4-methoxyphenyl)-3-oxopropanoate

: 1621392-91-3
C₂₀H₂₃NO₅

: C₂₀H₂₃NO₅

: 1621392-92-4
ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate

: C₂₀H₂₃NO₅

Guidance literature:: With [Cp*Ir(H₂O)((R)-8-amino-5,6,7,8-tetrahydroquinoline)]SO₄; sodium formate; In methanol; water; at 70 ℃; for 24h; Reagent/catalyst; stereoselective reaction; Catalytic behavior;
DOI:10.1016/j.tetasy.2014.06.003

Reference yield:

: 2881-83-6
ethyl 4-methoxybenzoylacetate

: 1621392-92-4
ethyl (2R,3S)-2-(benzamidomethyl)-3-hydroxy-3-(4-methoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 2 h / 0 - 20 °C

2: bis(1,5-cyclooctadiene)diiridium(I) dichloride; sodium acetate; hydrogen; C₃₉H₄₅FeN₂O₂PS / toluene; isopropyl alcohol / 24 h / 60 °C / 26601.8 Torr / Autoclave

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; boron trifluoride diethyl etherate; C₃₉H₄₅FeN₂O₂PS; hydrogen; sodium acetate; In dichloromethane; isopropyl alcohol; toluene;
DOI:10.1002/adsc.202100929