dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate

Base Information

Chemical Name:dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate
CAS No.:871332-30-8
Molecular Formula:C₂₄H₃₂N₈O₅
Molecular Weight:512.569
Hs Code.:

Synonyms:dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate

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Chemical Property of dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate

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Technology Process of dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate

There total 4 articles about dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 871332-22-8
4-({[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino)benzoic acid

: 32213-95-9
dimethyl L-aspartate hydrochloride

: 871332-30-8
dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield:

: 10541-83-0,937737-33-2
N-methyl-p-aminobenzoic acid

: 871332-30-8
dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / dimethylformamide / 12 h / 20 °C

2: 72 percent / diethyl cyanophosphonate; triethylamine / dimethylformamide / 12 h / 20 °C

With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide;

Reference yield:

: 74277-17-1
N-carbamimidoyl-3,5,5-trimethyl-4,5-dihydro-pyrazole-1-carboximidic acid amide

: 871332-30-8
dimethyl {4-[{[2-amino-4-(3,5,5-trimethylpyrazolin-2-yl)-1,3,5-triazin-6-yl]methyl}methylamino]benzoyl}-L-aspartate

Guidance literature:: Multi-step reaction with 3 steps

1: 26 percent / methanol / 2.5 h / 20 °C

2: 43 percent / dimethylformamide / 12 h / 20 °C

3: 72 percent / diethyl cyanophosphonate; triethylamine / dimethylformamide / 12 h / 20 °C

With diethyl cyanophosphonate; triethylamine; In methanol; N,N-dimethyl-formamide;