butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate

Base Information

Chemical Name:butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate
CAS No.:951671-26-4
Molecular Formula:C₂₄H₂₈F₃NO₃
Molecular Weight:435.486
Hs Code.:

Synonyms:butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate

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Chemical Property of butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate

Chemical Property:

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Technology Process of butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate

There total 5 articles about butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75091-99-5
4-(trifluoromethyl)cyclohexan-1-one

: 951671-26-4
butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 0 °C

1.2: 2 h / 0 °C

2.1: trifluorormethanesulfonic acid / 1.5 h / 0 °C

3.1: pyridine / dichloromethane

4.1: N-ethyl-N,N-diisopropylamine / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂

With pyridine; n-butyllithium; N-ethyl-N,N-diisopropylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; hexane; dichloromethane; trifluorormethanesulfonic acid;

Reference yield:

: C₂₀H₁₉F₆NO₄S

: 201230-82-2
carbon monoxide

: 71-36-3
butan-1-ol

: 951671-26-4
butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂;

Reference yield:

: 951671-25-3
4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]phenol

: 951671-26-4
butyl 4-[1-(6-methoxypyridin-3-yl)-4-(trifluoromethyl)cyclohexyl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane

2: N-ethyl-N,N-diisopropylamine / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂

With pyridine; N-ethyl-N,N-diisopropylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In dichloromethane;