methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside

Base Information Edit

Chemical Name:methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside
CAS No.:73541-94-3
Molecular Formula:C₂₆H₂₈O₅
Molecular Weight:420.505
Hs Code.:
Mol file:73541-94-3.mol

Synonyms:methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside

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Chemical Property of methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside Edit

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Technology Process of methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside

There total 8 articles about methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 76-83-5
trityl chloride

: 13145-22-7
methyl 2-deoxy-α-D-glucopyranoside

: 73541-94-3
methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside

Guidance literature:: With pyridine; for 16h; Ambient temperature;
DOI:10.1021/jo00195a023

Reference yield:

: 76-83-5
trityl chloride

: 73541-94-3
methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside

Guidance literature:: With pyridine; hydrogenchloride; potassium hydroxide; In diethyl ether; dichloromethane; pentane;

Reference yield:

: 102628-74-0
C₇H₁₃ClHgO₅

: 73541-94-3
methyl 2-deoxy-6-O-(triphenylmethyl)-α-D-arabinohexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaBH₄, 2.) 12N HCl / 1.) isopropanol-methanol, 0 deg C, 30 min, 2.) EtOAc

2: pyridine / 16 h / 23 °C

With hydrogenchloride; sodium tetrahydroborate; In pyridine;
DOI:10.1021/ja00524a046