cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-β-D-galactopyranoside

Base Information

• Chemical Name: cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-β-D-galactopyranoside
• CAS No.: 1206157-75-6
• Molecular Formula: C₅₇H₇₈O₆
• Molecular Weight: 859.243
• Mol file: 1206157-75-6.mol

Synonyms:cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-β-D-galactopyranoside

Chemical Property of cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-β-D-galactopyranoside

There total 2 articles about cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-C-acetyl-3,4,6-tri-O-benzyl-1,2-cyclopropane-1,2-deoxy-α-D-galactopyranose (1206157-59-6) + cholesterol (57-88-5) → cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-β-D-galactopyranoside (1206157-75-6)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at -20 - 20 ℃; Inert atmosphere; Molecular sieve;

DOI:10.1021/ol902732w

Reference yield:

1-C-acetyl-3,4,6-tri-O-benzyl-1,2-cyclopropane-1,2-deoxy-α-D-galactopyranose (1206157-59-6) + cholesterol (57-88-5) → cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-β-D-galactopyranoside (1206157-75-6) + cholesteryl 3,4,6-tri-O-benzyl-2-C-acetylmethyl-2-deoxy-α-D-galactopyranoside (1206157-74-5)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; Inert atmosphere; Molecular sieve;

DOI:10.1021/ol902732w

upstream raw materials:

1-C-acetyl-3,4,6-tri-O-benzyl-1,2-cyclopropane-1,2-deoxy-α-D-galactopyranose

cholesterol