N-phthaloyl-L-phenylalaninylnorleucine

Base Information

Chemical Name:N-phthaloyl-L-phenylalaninylnorleucine
CAS No.:138571-19-4
Molecular Formula:C₂₃H₂₄N₂O₅
Molecular Weight:408.454
Hs Code.:

Synonyms:N-phthaloyl-L-phenylalaninylnorleucine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phthaloyl-L-phenylalaninylnorleucine

Chemical Property:

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Technology Process of N-phthaloyl-L-phenylalaninylnorleucine

There total 3 articles about N-phthaloyl-L-phenylalaninylnorleucine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 138571-18-3
N-phthaloyl-L-phenylalanine-L-norleucine methyl ester

: 138571-19-4
N-phthaloyl-L-phenylalaninylnorleucine

Guidance literature:: With hydrogenchloride; In acetone; for 5h; Heating;
DOI:10.1021/jm00083a006

Reference yield:

: 3844-54-0
L-2-aminohexanoic acid-methyl ester hydrochloride

: 138571-19-4
N-phthaloyl-L-phenylalaninylnorleucine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triethylamine, N-hydroxybenzotriazole, 2.) 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / 1.) CH₂Cl₂, 2.) CH₂Cl₂, RT, overnight

2: 60 percent / aq. HCl / acetone / 5 h / Heating

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In acetone;
DOI:10.1021/jm00083a006

Reference yield:

: 5123-55-7
Nα-phthaloyl-L-phenylalanine

: 138571-19-4
N-phthaloyl-L-phenylalaninylnorleucine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triethylamine, N-hydroxybenzotriazole, 2.) 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / 1.) CH₂Cl₂, 2.) CH₂Cl₂, RT, overnight

2: 60 percent / aq. HCl / acetone / 5 h / Heating

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In acetone;
DOI:10.1021/jm00083a006