carbonic acid 1-[3-aminomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyf ester

Base Information

• Chemical Name: carbonic acid 1-[3-aminomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyf ester
• CAS No.: 1253421-29-2
• Molecular Formula: C₄₃H₇₁N₂O₁₀P
• Molecular Weight: 807.018

Synonyms:carbonic acid 1-[3-aminomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyf ester

Chemical Property of carbonic acid 1-[3-aminomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyf ester

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Technology Process of carbonic acid 1-[3-aminomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyf ester

There total 1 articles about carbonic acid 1-[3-aminomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyf ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

carbonic acid 1-[3-azidomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyl ester (1253421-28-1) → carbonic acid 1-[3-aminomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyf ester (1253421-29-2)

Guidance literature:

With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 48h;

Reference yield: 32.0%

[[11β,16α]-[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl] chloroformate (1253421-26-9) + carbonic acid 1-[3-aminomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyf ester (1253421-29-2) → [5-[1-[(tert-butoxycarbonyl)oxy]-2-[(t-butoxycarbonyl)-6-(4-phenylbutoxy)hexylamino]ethyl]-2-di-tert-butoxyphosphonooxybenzyl]carbamic acid [[11β,16α]-[16,17-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypreqna-1,4-diene-3,20-dion-21-yl]ester (1253421-30-5)

Guidance literature:

With 1,2,2,6,6-pentamethylpiperidine; In acetonitrile; at 20 ℃;

upstream raw materials:

carbonic acid 1-[3-azidomethyl-4-(di-tert-butoxyphosphoryloxy)phenyl]-2-[(tert-butoxycarbonyl)[6-(4-phenylbutoxy)hexyl]-amino]ethyl ester tert-butyl ester

Downstream raw materials:

[5-[1-[(tert-butoxycarbonyl)oxy]-2-[(t-butoxycarbonyl)-6-(4-phenylbutoxy)hexylamino]ethyl]-2-di-tert-butoxyphosphonooxybenzyl]carbamic acid [[11β,16α]-[16,17-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypreqna-1,4-diene-3,20-dion-21-yl]ester

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