5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene

Base Information

• Chemical Name: 5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene
• CAS No.: 109774-79-0
• Molecular Formula: C₆₉H₈₇N₇O₁₅S₆
• Molecular Weight: 1446.88

Synonyms:5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene

Chemical Property of 5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene

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Technology Process of 5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene

There total 4 articles about 5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

C30H33N3O6S3 (109774-71-2) + 6,6',6''-tritosyl-8,8',8''-nitrilotri(3-oxa-6-azaoctyl) tris(methanesulfonate) (98846-95-8) → 5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.13,25]heptatriaconta-1(26),2,25(37)-triene (109774-79-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 7h;

DOI:10.1016/S0040-4039(00)85349-6

Reference yield:

1,3,5-Tris(bromomethyl)benzene (18226-42-1) → 5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.13,25]heptatriaconta-1(26),2,25(37)-triene (109774-79-0)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium azide

2: LiAlH₄

4: 48 percent / Cs₂CO₃ / dimethylformamide / 7 h / 80 °C

With lithium aluminium tetrahydride; sodium azide; caesium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)85349-6

Reference yield:

1,3,5-tris(aminomethyl)benzene (77372-56-6) → 5,11,17,23,28,34-Hexakis-(toluene-4-sulfonyl)-8,20,31-trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.13,25]heptatriaconta-1(26),2,25(37)-triene (109774-79-0)

Guidance literature:

Multi-step reaction with 2 steps

2: 48 percent / Cs₂CO₃ / dimethylformamide / 7 h / 80 °C

With caesium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)85349-6

upstream raw materials:

C₃₀H₃₃N₃O₆S₃

6,6',6''-tritosyl-8,8',8''-nitrilotri(3-oxa-6-azaoctyl) tris(methanesulfonate)

1,3,5-Tris(bromomethyl)benzene

1,3,5-tris(aminomethyl)benzene

Downstream raw materials:

8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene; compound with toluene-4-sulfonic acid

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