8-Methyl-1h-benzo[d][1,3]oxazine-2,4-dione

Base Information

Chemical Name:8-Methyl-1h-benzo[d][1,3]oxazine-2,4-dione
CAS No.:66176-17-8
Molecular Formula:C9H7 N O3
Molecular Weight:177.159
Hs Code.:2934999090
European Community (EC) Number:672-320-4
DSSTox Substance ID:DTXSID60374956
Nikkaji Number:J2.401.026K
Wikidata:Q82163515

Synonyms:66176-17-8;8-methyl-1h-benzo[d][1,3]oxazine-2,4-dione;3-methylisatoic anhydride;3-Methyl-isatoic anhydride;8-methyl-2H-3,1-benzoxazine-2,4(1H)-dione;8-methyl-1H-3,1-benzoxazine-2,4-dione;8-methyl-2,4-dihydro-1H-3,1-benzoxazine-2,4-dione;MFCD03426399;3-methyl isatoic anhydride;8-methyl-1-H-benzo[d][1,3]oxazine-2,4-dione;SCHEMBL2060660;DTXSID60374956;CHKUQVBJPDLANA-UHFFFAOYSA-N;BBL104237;STK501275;3-Methylisatoic anhydride, AldrichCPR;AKOS000265330;CG-0740;A8937;CS-0034436;FT-0600655;VU0421928-2;8-Methyl-2H-3,1-benzooxazine-2,4(1H)-dione;EN300-7374687;Q-102107;F3223-0002;Z223648238;8-methyl-1H-benzo[d][1,3]oxazine-2,4-dione;3-METHYL-ISATOIC ANHYDRIDE

Suppliers and Price of 8-Methyl-1h-benzo[d][1,3]oxazine-2,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
8-Methyl-1H-benzo[d][1,3]oxazine-2,4-dione
100mg
$ 60.00

SynQuest Laboratories
3-Methylisatoic anhydride
25 g
$ 514.00

SynQuest Laboratories
3-Methylisatoic anhydride
1 g
$ 55.00

SynQuest Laboratories
3-Methylisatoic anhydride
5 g
$ 148.00

Matrix Scientific
8-Methyl-2H-3,1-benzoxazine-2,4(1H)-dione
500mg
$ 189.00

Crysdot
8-Methyl-1H-benzo[d][1,3]oxazine-2,4-dione 95+%
25g
$ 518.00

ChemScene
8-Methyl-1H-benzo[d][1,3]oxazine-2,4-dione >97.0%
5g
$ 113.00

ChemScene
8-Methyl-1H-benzo[d][1,3]oxazine-2,4-dione >97.0%
10g
$ 220.00

ChemScene
8-Methyl-1H-benzo[d][1,3]oxazine-2,4-dione >97.0%
25g
$ 400.00

AstaTech
3-METHYL-ISATOICANHYDRIDE 97%
25 / G
$ 450.00

Total 24 raw suppliers

Chemical Property of 8-Methyl-1h-benzo[d][1,3]oxazine-2,4-dione

Chemical Property:

Melting Point:207 °C
PKA:11.10±0.20(Predicted)
PSA：63.07000
Density:1.335g/cm³
LogP:0.78970
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:177.042593085
Heavy Atom Count:13
Complexity:251

Purity/Quality:

97% ^*data from raw suppliers

8-Methyl-1H-benzo[d][1,3]oxazine-2,4-dione ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi,Xn
Statements: 22-36
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C(=CC=C1)C(=O)OC(=O)N2

Technology Process of 8-Methyl-1h-benzo[d][1,3]oxazine-2,4-dione

There total 10 articles about 8-Methyl-1h-benzo[d][1,3]oxazine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75-44-5
phosgene

: 4389-45-1
3-methylantranilic acid

: 66176-17-8
6-methylisatoic anhydride

Guidance literature:: In 1,4-dioxane; benzene; Ambient temperature;
DOI:10.1021/jm00138a019

Reference yield: 95.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 4389-45-1
3-methylantranilic acid

: 66176-17-8
6-methylisatoic anhydride

Guidance literature:: In 1,4-dioxane; for 6.5h; Reflux;
DOI:10.1021/jf303376t

Reference yield: 94.0%

: 4389-45-1
3-methylantranilic acid

: 66176-17-8
6-methylisatoic anhydride

Guidance literature:: With bis(trichloromethyl) carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; for 16.5h;