4-hydroxyphenyl selenocyanide

Base Information

• Chemical Name: 4-hydroxyphenyl selenocyanide
• CAS No.: 77395-45-0
• Molecular Formula: C₇H₅NOSe
• Molecular Weight: 198.083
• Mol file: 77395-45-0.mol

Synonyms:4-hydroxyphenyl selenocyanide

Chemical Property of 4-hydroxyphenyl selenocyanide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-hydroxyphenyl selenocyanide

There total 6 articles about 4-hydroxyphenyl selenocyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4,4'-di(hydroxyphenyl)iodonium triflate + sodium selenocyanate (4768-87-0) → 4-hydroxyphenyl selenocyanide (77395-45-0)

Guidance literature:

With sodium triflate; In ethyl acetate; at 70 ℃; for 17h; Inert atmosphere;

DOI:10.1039/C8CC06211K

Reference yield: 87.0%

(p-hydroxyphenyl)boronic acid (71597-85-8) + potassium selenocyanate (3425-46-5) → 4-hydroxyphenyl selenocyanide (77395-45-0)

Guidance literature:

In acetonitrile; at 20 ℃; for 1.33333h; Electrochemical reaction;

Reference yield: 54.0%

C13H10N2O4S2Se + phenol (108-95-2,27073-41-2) → 4-hydroxyphenyl selenocyanide (77395-45-0)

Guidance literature:

In acetonitrile; at 20 ℃; for 0.333333h; Inert atmosphere; Sealed tube;

DOI:10.1055/a-1493-6885

upstream raw materials:

potassium selenocyanate

4-chloro-phenol

sodium selenocyanate

4-amino-phenol