5,20-diphenyl-10,15-di-p-tolyl-2-oxa-3-(2'-pyrrolyl)-21-carbaporphyrinato nickel(II)

Base Information

• Chemical Name: 5,20-diphenyl-10,15-di-p-tolyl-2-oxa-3-(2'-pyrrolyl)-21-carbaporphyrinato nickel(II)
• CAS No.: 628700-59-4
• Molecular Formula: C₅₀H₃₄N₄NiO
• Molecular Weight: 765.536

Synonyms:5,20-diphenyl-10,15-di-p-tolyl-2-oxa-3-(2'-pyrrolyl)-21-carbaporphyrinato nickel(II)

Chemical Property of 5,20-diphenyl-10,15-di-p-tolyl-2-oxa-3-(2'-pyrrolyl)-21-carbaporphyrinato nickel(II)

Chemical Property:

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Technology Process of 5,20-diphenyl-10,15-di-p-tolyl-2-oxa-3-(2'-pyrrolyl)-21-carbaporphyrinato nickel(II)

There total 1 articles about 5,20-diphenyl-10,15-di-p-tolyl-2-oxa-3-(2'-pyrrolyl)-21-carbaporphyrinato nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

5,20-diphenyl-10,15-di-p-tolyl-2-oxa-3-(2'-pyrrolyl)-21-carbaporphyrin + nickel dichloride (83864-14-6) → 5,20-diphenyl-10,15-di-p-tolyl-2-oxa-3-(2'-pyrrolyl)-21-carbaporphyrinato nickel(II) (628700-59-4)

Guidance literature:

With triethylamine; In methanol; chloroform; dissolving ligand in CHCl3 with NEt3, addn. of metal salt in methanol, stirring for 12 h; evapn., dissolving in CH2Cl2, filtration, chromy. (silica gel), recrystn. (CHCl3/methanol);

DOI:10.1021/ic051238x

upstream raw materials:

nickel dichloride

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