Technology Process of C61H73F3N2O20
There total 7 articles about C61H73F3N2O20 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1) CH3ONa, 2) toluene-4-sulfonic acid / 1) CH3OH, 2 h, 2) CH3CN, 50 deg C
2: pyridine / 20 h
3: NaBH3CN, HCl / tetrahydrofuran; diethyl ether / 8 h / 20 °C / molecular sieve 3 Angstroem
4: CH3ONa / methanol / 24 h
5: mercury cyanide / nitromethane; benzene / 2 h / 50 - 60 °C / molecular sieve 4 Angstroem
6: 1) ethyldiisopropylamine, (C2H5)4N(1+)*Br(1-) / 1) CH2Cl2, DMF, molecular sieve 4 Angstroem, 20 deg C, 15 h, 2) 96 h
With
pyridine; hydrogenchloride; tetraethylammonium bromide; sodium methylate; mercury(II) cyanide; sodium cyanoborohydride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; diethyl ether; nitromethane; benzene;
DOI:10.1007/BF00598177
- Guidance literature:
-
Multi-step reaction with 2 steps
1: mercury cyanide / nitromethane; benzene / 2 h / 50 - 60 °C / molecular sieve 4 Angstroem
2: 1) ethyldiisopropylamine, (C2H5)4N(1+)*Br(1-) / 1) CH2Cl2, DMF, molecular sieve 4 Angstroem, 20 deg C, 15 h, 2) 96 h
With
tetraethylammonium bromide; mercury(II) cyanide; N-ethyl-N,N-diisopropylamine;
In
nitromethane; benzene;
DOI:10.1007/BF00598177
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / 20 h
2: NaBH3CN, HCl / tetrahydrofuran; diethyl ether / 8 h / 20 °C / molecular sieve 3 Angstroem
3: CH3ONa / methanol / 24 h
4: mercury cyanide / nitromethane; benzene / 2 h / 50 - 60 °C / molecular sieve 4 Angstroem
5: 1) ethyldiisopropylamine, (C2H5)4N(1+)*Br(1-) / 1) CH2Cl2, DMF, molecular sieve 4 Angstroem, 20 deg C, 15 h, 2) 96 h
With
pyridine; hydrogenchloride; tetraethylammonium bromide; sodium methylate; mercury(II) cyanide; sodium cyanoborohydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; diethyl ether; nitromethane; benzene;
DOI:10.1007/BF00598177