3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:121042-73-7
Molecular Formula:C₂₀H₂₇F₃N₂O₇
Molecular Weight:464.439
Hs Code.:

Synonyms:3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Chemical Property:

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Technology Process of 3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 6 articles about 3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 121042-74-8
3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 121042-73-7
3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With methanol; sodium methylate; for 3h;
DOI:10.1016/j.carres.2016.09.016

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 121042-73-7
3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1) CH₃ONa, 2) toluene-4-sulfonic acid / 1) CH₃OH, 2 h, 2) CH₃CN, 50 deg C

2: pyridine / 20 h

3: NaBH₃CN, HCl / tetrahydrofuran; diethyl ether / 8 h / 20 °C / molecular sieve 3 Angstroem

4: CH₃ONa / methanol / 24 h

With pyridine; hydrogenchloride; sodium methylate; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1007/BF00598177

Reference yield:

: 121042-71-5
3-(trifluoroacetamido)propyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 121042-73-7
3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 20 h

2: NaBH₃CN, HCl / tetrahydrofuran; diethyl ether / 8 h / 20 °C / molecular sieve 3 Angstroem

3: CH₃ONa / methanol / 24 h

With pyridine; hydrogenchloride; sodium methylate; sodium cyanoborohydride; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1007/BF00598177