allyl (2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1-yl) carbonate

Base Information

Chemical Name:allyl (2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1-yl) carbonate
CAS No.:1401427-52-8
Molecular Formula:C₂₂H₂₁BrO₅
Molecular Weight:445.31
Hs Code.:

Synonyms:allyl (2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1-yl) carbonate

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Chemical Property of allyl (2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1-yl) carbonate

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Technology Process of allyl (2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1-yl) carbonate

There total 1 articles about allyl (2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1-yl) carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2749-70-4
bis(benzyloxy)methane

: 1401427-41-5
allyl (5-bromo-1-oxo-1,2,3,4-tetrahydronaphthalen-2-yl) carbonate

: 1401427-52-8
allyl (2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1-yl) carbonate

Guidance literature:: allyl (5-bromo-1-oxo-1,2,3,4-tetrahydronaphthalen-2-yl) carbonate; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

bis(benzyloxy)methane; With trimethylsilyl iodide; In tetrahydrofuran; at -78 ℃; for 0.583333h; Inert atmosphere;
DOI:10.1002/anie.201203663

Reference yield:

: 1401427-52-8
allyl (2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1-yl) carbonate

: 1401427-64-2
2-allyl-2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1(2H)-one

: 2-allyl-2-((benzyloxy)methoxy)-5-bromo-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (R,R)-ANDEN-phenyl Trost ligand; In tetrahydrofuran; at 20 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201203663