N-cyclohexyl-2,4-diaminoaniline

Base Information

• Chemical Name: N-cyclohexyl-2,4-diaminoaniline
• CAS No.: 21647-13-2
• Molecular Formula: C₁₂H₁₉N₃
• Molecular Weight: 205.303
• Mol file: 21647-13-2.mol

Synonyms:N-cyclohexyl-2,4-diaminoaniline

Chemical Property of N-cyclohexyl-2,4-diaminoaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-cyclohexyl-2,4-diaminoaniline

There total 1 articles about N-cyclohexyl-2,4-diaminoaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-cyclohexyl-2,4-dinitroaniline (52790-66-6) → N-cyclohexyl-2,4-diaminoaniline (21647-13-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1016/j.bmcl.2006.07.054

Reference yield:

N-cyclohexyl-2,4-diaminoaniline (21647-13-2) → 1-cyclohexyl-2-methyl-1H-benzoimidazol-5-ylamine (627469-68-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide

2: aq. HCl / 100 °C

With hydrogenchloride; triethylamine; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2006.07.054

Reference yield:

N-cyclohexyl-2,4-diaminoaniline (21647-13-2) → 6-(4-chloro-phenyl)-3-(1-cyclohexyl-2-methyl-1H-benzoimidazol-5-yl)-3H-thieno[3,2-d]pyrimidin-4-one

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N / dimethylformamide

2: aq. HCl / 100 °C

3: phenol / 110 - 130 °C

With hydrogenchloride; triethylamine; phenol; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2006.07.054

upstream raw materials:

N-cyclohexyl-2,4-dinitroaniline

Downstream raw materials:

1-cyclohexyl-2-methyl-1H-benzoimidazol-5-ylamine