(+)-(S_S)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

Base Information

• Chemical Name: (+)-(S_S)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine
• CAS No.: 864443-80-1
• Molecular Formula: C₂₃H₃₁NO₅S₂
• Molecular Weight: 465.635

Synonyms:(+)-(S_S)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

Chemical Property of (+)-(S_S)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

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Technology Process of (+)-(S_S)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

There total 1 articles about (+)-(S_S)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(+)-(SS)-S-methyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine + carbon dioxide (124-38-9,18923-20-1) → (+)-(SS)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine (864443-80-1)

Guidance literature:

(+)-(S_S)-S-methyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

carbon dioxide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

DOI:10.1021/jo050747d

Reference yield: 72.0%

(+)-(SS)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine (864443-80-1) + (2E)-3-phenyl-2-propen-1-ol (4407-36-7) → (+)-(SS)-S-phenyl-S-(3-phenyl-2-propenyloxycarboxymethyl)-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine (864443-87-8)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 16h;

DOI:10.1021/jo050747d

Reference yield: 72.0%

(+)-(SS)-S-carboxymethyl-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine (864443-80-1) + (Z)-2-hexen-1-ol (928-94-9) → (+)-(SS)-S-(2-Z-hexenyloxycarbonylmethyl)-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 16h;

DOI:10.1021/jo050747d

upstream raw materials:

carbon dioxide

Downstream raw materials:

(+)-(S_S)-S-(2-E-hexenyloxycarbonylmethyl)-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

(+)-(S_S)-S-(2-methyl-3-phenyl-2-propenyloxycarbonylmethyl)-S-phenyl-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

(+)-(S_S)-S-phenyl-S-[3-(4-nitrophenyl)-2-propenyloxycarboxymethyl]-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

(+)-(S_S)-S-phenyl-S-(3-phenyl-2-propenyloxycarboxymethyl)-N-(2,4,6-triisopropylphenylsulfonyl)sulfoximine

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