methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate

Base Information

Chemical Name:methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate
CAS No.:1192544-73-2
Molecular Formula:C₁₇H₂₅NO₆S
Molecular Weight:371.455
Hs Code.:

Synonyms:methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate

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Technology Process of methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate

There total 1 articles about methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 80657-57-4,42998-03-8
3-hydroxy-(2S)-methylpropionate

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 1192544-73-2
methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.07.060

Reference yield: 100.0%

: 1192544-73-2
methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate

: 1192544-74-3
tert-butyl (2S)-N-(3-hydroxy-2-methylpropyl)-N-(toluene-4-sulfonyl)carbamate

Guidance literature:: methyl (2S)-3-[N-(tert-butoxycarbonyl)-N-(4-methylphenylsulfonyl)]amino-2-methylpropanoate; With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1016/j.tet.2009.07.060