N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine

Base Information

Chemical Name:N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine
CAS No.:797762-99-3
Molecular Formula:C₃₀H₃₉NO₇S
Molecular Weight:557.708
Hs Code.:

Synonyms:N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine

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Technology Process of N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine

There total 6 articles about N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 98-59-9
p-toluenesulfonyl chloride

: 797762-98-2
N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxyethylamine

: 797762-99-3
N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine

Guidance literature:: With pyridine; at 20 ℃; for 20h;
DOI:10.3987/COM-04-10196

Reference yield:

: 100-39-0
benzyl bromide

: 797762-99-3
N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / K₂CO₃ / dimethylformamide / 48 h / 20 °C

2: benzene / 3 h / Heating

3: 9.69 g / NaBH₄ / methanol / 1 h / 20 °C

4: 88 percent / pyridine / 20 h / 20 °C

With pyridine; sodium tetrahydroborate; potassium carbonate; In methanol; N,N-dimethyl-formamide; benzene;
DOI:10.3987/COM-04-10196

Reference yield:

: 162976-09-2
2,4-diethoxy-3-methylphenol

: 797762-99-3
N-(2-benzyloxy-3,5-diethoxy-4-methylbenzyl)-2,2-dimethoxy-N-tosylethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 43 percent / acetic acid / 2 h / 135 - 145 °C

2: 98 percent / K₂CO₃ / dimethylformamide / 48 h / 20 °C

3: benzene / 3 h / Heating

4: 9.69 g / NaBH₄ / methanol / 1 h / 20 °C

5: 88 percent / pyridine / 20 h / 20 °C

With pyridine; sodium tetrahydroborate; potassium carbonate; In methanol; acetic acid; N,N-dimethyl-formamide; benzene; 1: Duff raction;
DOI:10.3987/COM-04-10196