4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone

Base Information

Chemical Name:4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone
CAS No.:223690-28-6
Molecular Formula:C₃₁H₄₀O₃Si
Molecular Weight:488.742
Hs Code.:

Synonyms:4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone

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Chemical Property of 4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone

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Technology Process of 4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone

There total 3 articles about 4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 223690-27-5
ethyl 5-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)-2-(2-naphthoyl)pentanoate

: 223690-28-6
4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone

Guidance literature:: With sodium hydroxide; In methanol; water; for 4h; Heating;
DOI:10.1246/bcsj.72.511

Reference yield:

: 62550-65-6
ethyl 2-naphthoylacetate

: 223690-28-6
4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaOEt; 18-crown-6 / ethanol / 3.5 h / 80 °C

2: 67 percent / NaOH / methanol; H₂O / 4 h / Heating

With sodium hydroxide; 18-crown-6 ether; sodium ethanolate; In methanol; ethanol; water; 1: Alkylation / 2: Decarboxylation;
DOI:10.1246/bcsj.72.511

Reference yield:

: 2-(3-bromopropyl)-1-methoxy-2-phenyl-1-(t-butyldimethylsilyloxy)cyclopropane

: 223690-28-6
4-(2-methoxy-1-phenyl-2-t-butyldimethylsilyloxy-cyclopropyl)butyl 2-naphthyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaOEt; 18-crown-6 / ethanol / 3.5 h / 80 °C

2: 67 percent / NaOH / methanol; H₂O / 4 h / Heating

With sodium hydroxide; 18-crown-6 ether; sodium ethanolate; In methanol; ethanol; water; 1: Alkylation / 2: Decarboxylation;
DOI:10.1246/bcsj.72.511