4-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

Base Information

Chemical Name:4-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER
CAS No.:303041-88-5
Molecular Formula:C14H14 Br N O3
Molecular Weight:324.17
Hs Code.:2933990090
Mol file:303041-88-5.mol

Synonyms:4-BROMOINDOLE-3-CARBOXALDEHYDE, N-BOC PROTECTED;4-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;4-BROMO-3-FORMYLINDOLE, N-BOC PROTECTED;4-Bromo-1H-indole-3-carboxaldehyde, N-BOC protected 98%;4-Bromo-3-formyl-1H-indole, N-BOC protected;tert-butyl 4-bromo-3-formyl-1H-indole-1-carboxylate;4-Bromo-1H-indole-3-carboxaldehyde, N-BOC protected

Suppliers and Price of 4-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-Boc-4-Bromo-3-formylindole
500mg
$ 130.00

SynQuest Laboratories
4-Bromo-1H-indole-3-carboxaldehyde, N-Boc protected 98%
5 g
$ 202.00

SynQuest Laboratories
4-Bromo-1H-indole-3-carboxaldehyde, N-Boc protected 98%
1 g
$ 63.00

SynChem
4-Bromo-3-formylindole-1-carboxylic acid tert-butyl ester 95%
5 g
$ 300.00

SynChem
4-Bromo-3-formylindole-1-carboxylic acid tert-butyl ester 95%
1 g
$ 100.00

Matrix Scientific
1-Boc-4-Bromo-3-formylindole 95+%
1g
$ 231.00

Matrix Scientific
1-Boc-4-Bromo-3-formylindole 95+%
5g
$ 648.00

Matrix Scientific
1-Boc-4-Bromo-3-formylindole 95+%
10g
$ 893.00

Labseeker
tert-butyl4-bromo-3-formyl-1H-indole-1-carboxylate 95
25g
$ 2567.00

Crysdot
1-Boc-4-Bromo-3-formylindole 95+%
25g
$ 781.00

Total 26 raw suppliers

Chemical Property of 4-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

Chemical Property:

Vapor Pressure:1.73E-07mmHg at 25°C
Boiling Point:426.7°Cat760mmHg
Flash Point:211.9°C
PSA：48.30000
Density:1.42g/cm³
LogP:3.99950
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1-Boc-4-Bromo-3-formylindole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

There total 3 articles about 4-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 98600-34-1
4-bromo-1H-indole-3-carbaldehyde

: 303041-88-5
4-bromo-1-tert-butoxycarbonylindole-3-carboxaldehyde

Guidance literature:: With dmap; In acetonitrile; Inert atmosphere;
DOI:10.1021/acs.joc.5b02815

Reference yield: 95.0%

: 303041-88-5
4-bromo-1-tert-butoxycarbonylindole-3-carboxaldehyde

Guidance literature:: With dmap; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

Reference yield:

: 52488-36-5
4-bromo-1H-indole

: 303041-88-5
4-bromo-1-tert-butoxycarbonylindole-3-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 0 - 20 °C

1.2: Reflux

2.1: dmap / acetonitrile

With dmap; trichlorophosphate; In acetonitrile;
DOI:10.1021/ol4025259