2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide

Base Information

Chemical Name:2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide
CAS No.:916993-79-8
Molecular Formula:C₂₂H₃₁N₃O₃
Molecular Weight:385.506
Hs Code.:

Synonyms:2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide

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Chemical Property of 2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide

Chemical Property:

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Technology Process of 2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide

There total 3 articles about 2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 118-48-9
isatoic anhydride

: 127404-85-7
N-<2-(3,4-dimethoxyphenyl)ethyl>-N-methyl-1,4-butanediamine

: 916993-79-8
2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide

Guidance literature:: In acetonitrile; for 18h; Heating;
DOI:10.1016/j.bmc.2006.07.055

Reference yield:

: 916993-74-3
4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butanenitrile

: 916993-79-8
2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaOH; hydrogen; nickel / ethanol / 12 h / 2068.59 Torr

2: 80 percent / acetonitrile / 18 h / Heating

With sodium hydroxide; hydrogen; nickel; In ethanol; acetonitrile;
DOI:10.1016/j.bmc.2006.07.055

Reference yield:

: 3490-06-0
N-methylhomoveratrylamine

: 916993-79-8
2-amino-N-{4-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]butyl}benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / sodium carbonate; sodium iodide / 2-methyl-propan-2-ol / 24 h / Heating

2: 91 percent / NaOH; hydrogen; nickel / ethanol / 12 h / 2068.59 Torr

3: 80 percent / acetonitrile / 18 h / Heating

With sodium hydroxide; hydrogen; nickel; sodium carbonate; sodium iodide; In ethanol; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmc.2006.07.055