1,3-bis(dimethylgallyl)benzene

Base Information

Chemical Name:1,3-bis(dimethylgallyl)benzene
CAS No.:1147093-99-9
Molecular Formula:C₁₀H₁₆Ga₂
Molecular Weight:275.683
Hs Code.:

Synonyms:1,3-bis(dimethylgallyl)benzene

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Chemical Property of 1,3-bis(dimethylgallyl)benzene

Chemical Property:

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Technology Process of 1,3-bis(dimethylgallyl)benzene

There total 1 articles about 1,3-bis(dimethylgallyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 89379-58-8
1,3-bis(chloromercurio)benzene

: 1445-79-0
trimethyl gallium

: 1147093-99-9
1,3-bis(dimethylgallyl)benzene

Guidance literature:: In neat (no solvent); byproducts: HgMe2, Me2GaCl; (Ar); std. Schlenk technique; suspn. of Hg compd. and Me3Ga was heated at 120°C for 7 h; cooled without stirring to 40°C overnight; septd. by syringe; residue washed (hexane); dried (vac., 3 h);
DOI:10.1021/om900048c

Reference yield:

: 1147093-99-9
1,3-bis(dimethylgallyl)benzene

: 1445-79-0
trimethyl gallium

Guidance literature:: In neat (no solvent); (Ar); std. Schlenk technique; 2 flask were connected by bent ground-glass joint; flask with Ga compd. was evacuated (0.1 mbar) and heated at 120°C for 30 min; another flask was cooled with liq. N2; NMR monitoring;
DOI:10.1021/om900048c

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1147093-99-9
1,3-bis(dimethylgallyl)benzene

: trimethylgallium - THF

: bis(3-dimethylgallylphenyl*THF)methylgallium*THF

Guidance literature:: In tetrahydrofuran; benzene-d6; (Ar); std. Schlenk technique; Ga compd. was dissolved in C6D6/THF (1/1); NMR monitoring;
DOI:10.1021/om900048c