C₃₁H₄₇OP

Base Information

Chemical Name:C₃₁H₄₇OP
CAS No.:1026348-52-6
Molecular Formula:C₃₁H₄₇OP
Molecular Weight:466.687
Hs Code.:

Synonyms:C₃₁H₄₇OP

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Chemical Property of C₃₁H₄₇OP

Chemical Property:

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Technology Process of C₃₁H₄₇OP

There total 7 articles about C₃₁H₄₇OP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1027163-63-8
Methanesulfonic acid (S)-1-[2-(diphenyl-phosphinoyl)-ethyl]-heptadecyl ester

: 1026348-52-6
C₃₁H₄₇OP

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(97)01234-3

Reference yield:

: 603-35-0
triphenylphosphine

: 1026348-52-6
C₃₁H₄₇OP

Guidance literature:: Multi-step reaction with 4 steps

1: CaCO₃ / acetonitrile / 80 °C

2: 744 mg / NaOH / tetrahydrofuran; H₂O / 2 h / 50 °C

3: 100 percent / triethylamine / CH₂Cl₂ / 0.25 h / 0 °C

4: 87 percent / sodium bis(trimethylsilyl)amide / tetrahydrofuran; toluene / 0.25 h / 0 °C

With sodium hydroxide; sodium hexamethyldisilazane; triethylamine; calcium carbonate; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;
DOI:10.1016/S0040-4020(97)10099-0

Reference yield:

: (S)-Nonadecane-1,3-diol

: 1026348-52-6
C₃₁H₄₇OP

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / hexamethylphosphoric triamide, iodine, triphenylphosphine / toluene / 1.5 h / Ambient temperature

2: CaCO₃ / acetonitrile / 80 °C

3: 744 mg / NaOH / tetrahydrofuran; H₂O / 2 h / 50 °C

4: 100 percent / triethylamine / CH₂Cl₂ / 0.25 h / 0 °C

5: 87 percent / sodium bis(trimethylsilyl)amide / tetrahydrofuran; toluene / 0.25 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; iodine; sodium hexamethyldisilazane; triethylamine; triphenylphosphine; calcium carbonate; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;
DOI:10.1016/S0040-4020(97)10099-0