((3R,4S,5R)-2-benzyl-5-methyl-3-phenylisoxazolidin-4-yl)(1-methyl-1H-imidazol-2-yl)methanone

Base Information

Chemical Name:((3R,4S,5R)-2-benzyl-5-methyl-3-phenylisoxazolidin-4-yl)(1-methyl-1H-imidazol-2-yl)methanone
CAS No.:906792-93-6
Molecular Formula:C₂₂H₂₃N₃O₂
Molecular Weight:361.444
Hs Code.:

Synonyms:((3R,4S,5R)-2-benzyl-5-methyl-3-phenylisoxazolidin-4-yl)(1-methyl-1H-imidazol-2-yl)methanone

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Chemical Property of ((3R,4S,5R)-2-benzyl-5-methyl-3-phenylisoxazolidin-4-yl)(1-methyl-1H-imidazol-2-yl)methanone

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Technology Process of ((3R,4S,5R)-2-benzyl-5-methyl-3-phenylisoxazolidin-4-yl)(1-methyl-1H-imidazol-2-yl)methanone

There total 2 articles about ((3R,4S,5R)-2-benzyl-5-methyl-3-phenylisoxazolidin-4-yl)(1-methyl-1H-imidazol-2-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 860772-38-9
(E)‐1‐(1‐methyl‐1H‐imidazole‐2‐yl)‐but‐2‐en‐1‐one

: 3376-26-9
N-Benzylidenebenzylamine N-oxide

: 906792-93-6
((3R,4S,5R)-2-benzyl-5-methyl-3-phenylisoxazolidin-4-yl)(1-methyl-1H-imidazol-2-yl)methanone

Guidance literature:: With 4 A molecular sieve; chiral bis(oxazolinyl)pyridine-cerium(IV) triflate; In ethyl acetate; at 0 ℃; for 17h;
DOI:10.1021/ol061223i

Reference yield:

: 103-49-1
dibenzylamine

: 906792-93-6
((3R,4S,5R)-2-benzyl-5-methyl-3-phenylisoxazolidin-4-yl)(1-methyl-1H-imidazol-2-yl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Na₂WO₄*2H₂O; H₂O₂ / H₂O / 3 h / 0 - 20 °C

2: 99 percent / molecular sieves 4 Angstroem / chiral bis(oxazolinyl)pyridine-cerium(IV) triflate complex / ethyl acetate / 17 h / 0 °C

With sodium tungstate; 4 A molecular sieve; dihydrogen peroxide; chiral bis(oxazolinyl)pyridine-cerium(IV) triflate; In water; ethyl acetate;
DOI:10.1021/ol061223i