tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate

Base Information

Chemical Name:tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate
CAS No.:1233122-88-7
Molecular Formula:C₂₄H₄₅NO₇P₂
Molecular Weight:521.571
Hs Code.:

Synonyms:tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate

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Chemical Property of tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate

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Technology Process of tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate

There total 5 articles about tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 926026-55-3
tetraethyl 3-oxopropane-1,1-diyldiphosphonate

: 1021204-99-8
5-(benzyloxy)-N-methylpentan-1-amine

: 1233122-88-7
tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate

Guidance literature:: With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1039/b9nj00597h

Reference yield:

: 17053-10-0
[2-(1,3-dioxolan-2-yl)ethyl]phosphonic acid diethyl ester

: 1233122-88-7
tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 20 °C

1.2: 1 h / -78 °C

2.1: hydrogenchloride / water; acetone / 3 h / 50 °C

3.1: sodium tris(acetoxy)borohydride / dichloromethane / 4 h / 20 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; sodium tris(acetoxy)borohydride; In tetrahydrofuran; hexane; dichloromethane; water; acetone;
DOI:10.1039/b9nj00597h

Reference yield:

: 926026-53-1
tetraethyl 2-(1,3-dioxolan-2-yl)ethane-1,1-dilydiphosphonate

: 1233122-88-7
tetraethyl 3-((5-(benzyloxy)pentyl)(methyl)amino)propane-1,1-diyldiphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water; acetone / 3 h / 50 °C

2: sodium tris(acetoxy)borohydride / dichloromethane / 4 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium tris(acetoxy)borohydride; In dichloromethane; water; acetone;
DOI:10.1039/b9nj00597h