C₅₅H₃₈N₂Si

Base Information

Chemical Name:C₅₅H₃₈N₂Si
CAS No.:1262867-04-8
Molecular Formula:C₅₅H₃₈N₂Si
Molecular Weight:755.006
Hs Code.:

C<sub>55</sub>H<sub>38</sub>N<sub>2</sub>Si

Synonyms:C₅₅H₃₈N₂Si

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Chemical Property of C₅₅H₃₈N₂Si

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Technology Process of C₅₅H₃₈N₂Si

There total 5 articles about C₅₅H₃₈N₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.14%

: 76-86-8
Triphenylsilyl chloride

: 1262867-03-7
C₃₇H₂₃BrN₂

: 1262867-04-8
C₅₅H₃₈N₂Si

Guidance literature:: C₃₇H₂₃BrN₂; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

Triphenylsilyl chloride; In tetrahydrofuran; hexane; at 20 ℃; for 12h;

Reference yield:

: 205-25-4
benzo[c]carbazole

: 1262867-04-8
C₅₅H₃₈N₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / copper(l) iodide; trans-1,2-cyclohexanediamine / dichlorobenzene, 1,2- / 12 h / 180 °C

2.1: potassium phosphate / palladium diacetate; tri-tert-butyl phosphine / toluene; 1,4-dioxane / 5 h / 100 °C

3.1: N-Bromosuccinimide / tetrahydrofuran / 12 h / 20 °C

4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

4.2: 12 h / 20 °C

With potassium phosphate; N-Bromosuccinimide; n-butyllithium; caesium carbonate; copper(l) iodide; tri-tert-butyl phosphine; palladium diacetate; trans-1,2-cyclohexanediamine; In tetrahydrofuran; 1,4-dioxane; dichlorobenzene, 1,2-; hexane; toluene;

Reference yield:

: 13922-41-3
1-Naphthylboronic acid

: 1262867-04-8
C₅₅H₃₈N₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 4 h / 100 °C

2.1: triethyl phosphite / dichlorobenzene, 1,2- / 12 h / 150 °C

3.1: caesium carbonate / copper(l) iodide; trans-1,2-cyclohexanediamine / dichlorobenzene, 1,2- / 12 h / 180 °C

4.1: potassium phosphate / palladium diacetate; tri-tert-butyl phosphine / toluene; 1,4-dioxane / 5 h / 100 °C

5.1: N-Bromosuccinimide / tetrahydrofuran / 12 h / 20 °C

6.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

6.2: 12 h / 20 °C

With potassium phosphate; N-Bromosuccinimide; n-butyllithium; potassium carbonate; caesium carbonate; triethyl phosphite; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; trans-1,2-cyclohexanediamine; In tetrahydrofuran; 1,4-dioxane; dichlorobenzene, 1,2-; ethanol; hexane; toluene;