2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate

Base Information

• Chemical Name: 2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate
• CAS No.: 1005001-05-7
• Molecular Formula: C₁₆H₁₈N₂O₆
• Molecular Weight: 334.329

Synonyms:2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate

Chemical Property of 2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate

Chemical Property:

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Technology Process of 2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate

There total 1 articles about 2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

di(succinimido) carbonate (74124-79-1) + N-benzylidene-1-hydroxy-2-methyl-2-propanamine N-oxide (55277-95-7) → 2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate (1005001-05-7)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃; for 16h;

DOI:10.1002/chem.200700369

Reference yield: 46.0%

6-monodeoxy-6-monoamino-(2,3-di-O-methyl)-hexakis(2,3,6-tri-O-methyl)-β-cyclodextrin hydrochloride + 2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate (1005001-05-7) → mono(6-(2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide)-ethylenecarbamoyl-6-deoxy-2,3-O-methyl)-hexakis(2,3,6-tri-O-methyl)-β-cyclodextrin (1005032-13-2)

Guidance literature:

With triethylamine; In dichloromethane; for 6h;

DOI:10.1002/chem.200700369

Reference yield: 19.0%

2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide succinimidyl carbonate (1005001-05-7) + 6-monodeoxy-6-monoamino-(2-O-methyl)-hexakis(2,6-di-O-methyl)-β-cyclodextrin hydrochloride (1005001-06-8) → mono(6-(2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide)-ethylenecarbamoyl-6-deoxy-2-O-methyl)-hexakis(2,6-di-O-methyl)-β-cyclodextrin (1005001-07-9)

Guidance literature:

With triethylamine; In dichloromethane; for 1h;

DOI:10.1002/chem.200700369

upstream raw materials:

di(succinimido) carbonate

N-benzylidene-1-hydroxy-2-methyl-2-propanamine N-oxide

Downstream raw materials:

mono(6-(2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide)-ethylenecarbamoyl-6-deoxy-2,3-O-methyl)-hexakis(2,3,6-tri-O-methyl)-β-cyclodextrin

mono(6-(2,2-dimethyl-2-[(phenylmethylene)amino] N-oxide)-ethylenecarbamoyl-6-deoxy-2-O-methyl)-hexakis(2,6-di-O-methyl)-β-cyclodextrin

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