O,O,O-tris(p-chlorophenyl) phosphorothioate

Base Information

• Chemical Name: O,O,O-tris(p-chlorophenyl) phosphorothioate
• CAS No.: 3071-56-5
• Molecular Formula: C₁₈H₁₂Cl₃O₃PS
• Molecular Weight: 445.69

Synonyms:O,O,O-tris(p-chlorophenyl) phosphorothioate

Chemical Property of O,O,O-tris(p-chlorophenyl) phosphorothioate

Chemical Property:

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Technology Process of O,O,O-tris(p-chlorophenyl) phosphorothioate

There total 11 articles about O,O,O-tris(p-chlorophenyl) phosphorothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4-chloro-phenol (106-48-9,82344-39-6) → O,O,O-tris(p-chlorophenyl) phosphorothioate (3071-56-5)

Guidance literature:

With sodium hydroxide; Aliquat 336; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1021/je00048a038

Reference yield: 85.0%

4-chloro-phenol (106-48-9,82344-39-6) → O,O,O-tris(p-chlorophenyl) phosphorothioate (3071-56-5)

Guidance literature:

With sodium hydroxide; trichlorophosphate; PEG-400; In chloroform; water; at 20 ℃; for 3h;

Reference yield: 60.0%

4-chloro-phenol (106-48-9,82344-39-6) → O,O,O-tris(p-chlorophenyl) phosphorothioate (3071-56-5) + tetrakis(p-chlorophenoxy)diphosphine disulfide (73608-50-1)

Guidance literature:

With phosphorus; sulfur; at 150 - 217 ℃; for 8.5h;

upstream raw materials:

tris(p-chlorophenyl)phosphite

sodium 4-chlorophenolate

4-chloro-phenol

5-phenyl-3H-1,2,4-dithiazole-3-one

Downstream raw materials:

diethyl-amidothiophosphoric acid O,O'-bis-(4-chloro-phenyl ester)

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