C₄₉H₅₃F₃N₈O₉

Base Information

Chemical Name:C₄₉H₅₃F₃N₈O₉
CAS No.:1349029-02-2
Molecular Formula:C₄₉H₅₃F₃N₈O₉
Molecular Weight:955.003
Hs Code.:

C<sub>49</sub>H<sub>53</sub>F<sub>3</sub>N<sub>8</sub>O<sub>9</sub>

Synonyms:C₄₉H₅₃F₃N₈O₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₉H₅₃F₃N₈O₉

Chemical Property:

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Technology Process of C₄₉H₅₃F₃N₈O₉

There total 19 articles about C₄₉H₅₃F₃N₈O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1349028-89-2
C₁₇H₁₈F₃N₅O₃

: 1349029-01-1
C₃₂H₃₇N₃O₇

: 1349029-02-2
C₄₉H₅₃F₃N₈O₉

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 261952-01-6
4-methyl-3-(trifluoromethyl)benzoic acid

: 1349029-02-2
C₄₉H₅₃F₃N₈O₉

Guidance literature:: Multi-step reaction with 8 steps

1: sulfuric acid / 12 h / Reflux

2: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 24 h / Reflux

3: ammonia / methanol

4: triethylamine / dichloromethane

5: water; lithium hydroxide / tetrahydrofuran; methanol

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran

7: N-ethyl-N,N-diisopropylamine; ammonia / isopropyl alcohol / 12 h

8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

With dmap; N-Bromosuccinimide; ammonia; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; sulfuric acid; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; isopropyl alcohol;

Reference yield:

: 103440-52-4
methyl 2-iodo-5-methylbenzoate

: 1349029-02-2
C₄₉H₅₃F₃N₈O₉

Guidance literature:: Multi-step reaction with 7 steps

1: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 24 h / Reflux

2: 0.33 h / Microwave irradiation

3: triethylamine / dichloromethane

4: potassium acetate / palladium diacetate; 1,1'-bis-(diphenylphosphino)ferrocene / dimethyl sulfoxide / 0.5 h

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

6: water; lithium hydroxide / tetrahydrofuran; methanol

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

With dmap; N-Bromosuccinimide; water; potassium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; dimethyl sulfoxide;