Technology Process of C29H35N5O9
There total 16 articles about C29H35N5O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C29H37N5O10;
With
diethylamino-sulfur trifluoride;
In
dichloromethane;
at -78 ℃;
for 4h;
With
potassium carbonate;
In
dichloromethane;
at -78 ℃;
- Guidance literature:
-
C29H37N5O10;
With
diethylamino-sulfur trifluoride;
In
dichloromethane;
at -78 ℃;
for 4h;
With
potassium carbonate;
In
dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogen / palladium(II) hydroxide/carbon / methanol / 72 h / 2068.65 Torr
2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
3.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C
4.1: 2,6-dimethylpyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C
5.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 18 h / 20 °C
6.1: diethylamino-sulfur trifluoride / dichloromethane / 4 h / -78 °C
6.2: -78 °C
With
pyridine; 1H-imidazole; 2,6-dimethylpyridine; diethylamino-sulfur trifluoride; hydrogen; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
palladium(II) hydroxide/carbon;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;